What is it about?
NMR is a well established technique utilized by chemists the world over to elucidate chemical structures. The majority of chemists at this point are used to 1H and 13C NMR and a small array of 2D experiments. Many are not aware of how 15N NMR, despite the nucleus being a very rare spin, is now accessible with modern NMR techniques, especially via indirect techniques. This chapter discusses various aspects of applying experimental AND predictive N15NMR to alkaloid structure elucidation
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Why is it important?
For scientists interested in understanding how N15 NMR can be used for structure elucidation of complex compounds this would be a good general review of how it is applied to natural products
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Read the Original
This page is a summary of: Applications of15N NMR Spectroscopy in Alkaloid Chemistry, October 2007, Wiley,
DOI: 10.1002/9783527621071.ch14.
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Resources
Long-range 1H-15N heteronuclear shift correlation
The investigation of long-range 1H–15N heteronuclear shift correlation NMR experiments has gone from its inception in 1995 to a robust area of research with numerous studies now reported annually. The area has been reviewed twice, covering the literature through about mid-2000. The present report covers the period from where this author's previous review stopped in late-1999 through the present. New long-range heteronuclear shift correlation methods that are applicable to long-range 1H–15N 2D he
Chapter Summary on the Wiley website
The WIley webpage regarding the book chapter
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